Τίτλος:
A convenient one-step synthesis of stable β-amino alcohol N-boranes from α-amino acids
Γλώσσες Τεκμηρίου:
Αγγλικά
Περίληψη:
Novel, non-cyclic -amino alcohol N-boranes are isolated from the sodium borohydride-sulfuric acid assisted direct reduction of a series of -amino acids. The reduction takes place in one step under mild conditions and affords the products in good yields. © Georg Thieme Verlag Stuttgart · New York.
Συγγραφείς:
Georgios Vougioukalakis
Kyriakos Papadopoulos
Afroditi Pinaka
Dimitra Dimotikali
Vassilis Psyharis
Περιοδικό:
SYNTHESE - DORDRECHT
Εκδότης:
Georg Thieme Verlag KG
Λέξεις-κλειδιά:
-amino alcohol N -boranes; Amino alcohols; Direct Reduction; Good yield; One step; One step synthesis; sodium borohydride, Amines; Amino acids; Boron compounds; Hydrides; Reduction; Sodium; Sulfuric acid, Alcohols, 2 amino 2 phenylethanol n borane; 2 amino 3 (1h indol 2 yl)propan 1 ol n borane; 2 amino 3 methylpentan 1 ol n borane; 2 amino 3 phenylpropan 1 ol n borane; 2 amino 4 methylpentan 1 ol n borane; 2 amino 4 methylsulfanylbutan 1 ol n borane; alpha amino acid; aminoalcohol; borane derivative; isoleucine; leucine; methionine; phenylalanine; phenylglycine; sodium borohydride; sulfuric acid; tryptophan; unclassified drug, article; carbon nuclear magnetic resonance; chemical structure; heteronuclear single quantum coherence; infrared spectroscopy; mass spectrometry; proton nuclear magnetic resonance; synthesis; X ray crystallography
Κύρια θεματική κατηγορία:
Θετικές Επιστήμες
DOI:
10.1055/s-0031-1289727
