Τίτλος:
Refinement of
2-amino-6-(4-methyl-1-piperazinyl)-4-(tricyclo[3.3.1.1(3,7)]dec-1-yl)-
1,3,5-triazine at three different temperatures using image-plate data
Γλώσσες Τεκμηρίου:
Αγγλικά
Περίληψη:
The structure of
2-amino-6-(4-methyl-1-piperazinyl)-4-(tricyclo[3.3.1.1
(3,7)]dec-1-yl)-1,3,5-triazine was refined using data collected at three
different temperatures [room temperature (293 K), 150 K and 85 K] with
the use of an image-plate scanner in an attempt to study the effect of
temperature on the disorder of the adamantyl group. It is demonstrated
that the data collected with the rotation method and an image-plate
scanner are of a high enough quality to be used for the refinement of
small-molecule structures.
Συγγραφείς:
Perrakis, A
Schneider, TR
AntoniadouVyzas, E
Dauter, Z and
Hamodrakas, SJ
Περιοδικό:
Journal of Applied Crystallography
Εκδότης:
MUNKSGAARD INT PUBL LTD
DOI:
10.1107/S0021889896000180
